基于分段涂层TDR-两电极法联合的含水合物多孔介质宽频电学参数测试仿真研究
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中国石油大学华东 控制科学与工程学院

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国家科技重大专项(2024ZD140660408);国家留学基金项目(202106455003);山东省自然科学基金项目(ZR2024ME090);中石油“十四五”前瞻性基础性重大科技项目(2024DJ9601);三亚市“崖州湾”菁英人才科技专项项目(SCKJ-JYRC-2023-06)


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    摘要:

    含水多孔介质在不同频段主导极化机制的差异导致介电常数发生频散,宽频段介电常数谱蕴含了多孔介质的多尺度结构特性及组分含量等重要信息。电磁波时域反射法(TDR)适用于MHz~GHz频段、电极法适用于MHz以下的频段,然而TDR探头和电极法中电极的结构差异导致两者的测试对象不一致,所以测试数据无法联合解释。针对含水合物海洋沉积物的宽频电学参数测试需求提出了一种基于分段涂层TDR法和两电极法联合的测试新方案。设计了内嵌式分段涂层TDR探头并建立了用于TDR仿真测试的有限元数值模型,设计正交实验确定了涂层最优参数为间隙数量3、间隙长度2mm、涂层厚度0.5mm。建立了用于两电极法仿真测试的有限元数值模型,确定了用以将电阻抗转换为复电导率的探头几何因子;根据仿真数据建立了针对内嵌式分段涂层影响的电学参数测量值校正模型。以不同水合物饱和度条件下的多孔介质为被测对象开展TDR-两电极法联合仿真测试,获得了宽频段(mHz~GHz)电学参数。结果表明:利用TDR法测量得到的高频介电常数和电导率均随水合物饱和度的增大而减小,校正后的平均相对误差分别为2.44%和6.22%;利用两电极法测量得到低频等效介电常数随水合物饱和度的增大而减小,在双电层极化主导的频段校正后平均相对误差为2.20%。该研究成果为将来开发含水合物海洋沉积物宽频电学参数测试实验装置提供了理论和技术支撑。

    Abstract:

    The differences in dominant polarization mechanisms of water-bearing porous media across various frequency bands lead to dispersion in the dielectric permittivity. The broadband dielectric spectrum contains critical information about the multiscale structural characteristics and component contents of the porous medium. Time-domain reflectometry (TDR) is suitable for MHz to GHz frequencies, while the electrode-based method is applicable to frequencies below MHz. However, due to structural differences between TDR probes and electrodes, their testing targets are inconsistent, making it impossible to jointly interpret test data. To address the requirement for broadband electrical parameter testing of hydrate-bearing marine sediments, a novel testing scheme combining segmented-coating TDR and two-electrode methods was proposed. A new embedded- and segmented-coating TDR probe was designed, and a finite element numerical model was established. Orthogonal experiments were conducted and the optimal parameters were obtained, i.e., 3 gaps with the lengths of 2mm and the coating with the thickness of 0.5mm. A finite element numerical model for the two-electrode method was developed, and numerical simulations were conducted to determine the probe's geometric factor for converting impedance into complex conductivity. Correction models for measured values influenced by embedded- and segmented-coating were established for conductivity and dielectric permittivity measurements. Simulation tests based on the joint TDR and two-electrode methods were performed on porous media under different hydrate saturations using the same probe to achieve broadband (mHz-GHz) electrical parameter testing. Simulation results show that both the high-frequency dielectric permittivity and conductivity measured by the TDR method decrease with increasing hydrate saturation, with the average relative errors of 2.44% and 6.22%, respectively. The low-frequency equivalent dielectric permittivity measured by the two-electrode method also decrease with increasing hydrate saturation, with the average relative error of 2.20% in the frequency band dominated by electrical-double-layer polarization. This research provides a theoretical and technical support for the future development of experimental apparatus for measuring broadband electrical parameters of hydrate-bearing marine sediments.

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王永辉,邢兰昌,朱作飞,魏伟,韩维峰,王云龙,武晓菲.基于分段涂层TDR-两电极法联合的含水合物多孔介质宽频电学参数测试仿真研究计算机测量与控制[J].,2025,33(10):55-63.

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  • 收稿日期:2025-04-27
  • 最后修改日期:2025-06-06
  • 录用日期:2025-06-09
  • 在线发布日期: 2025-10-27
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